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Most of these are going to be Whole-genome sequencing of some model organism:en.wikipedia.org/wiki/Whole_genome_sequencing#History lists them all. Basically th big "firsts" all happened in the 1990s and early 2000s.
- 2003: Human Genome Project (3 Gbp)
Big excitement picture at: molecular biology technologies.
A concrete experiment has been done at Section "Sequencing" on section sequencing.